Lecture Advanced NMR Spectroscopy                          TUMonline

Vorlesung, 3 SWS / 5 ECTS; Chemie (M.Sc.): Schwerpunkt OC (Wahlpflicht), alle HF/NF (Wahlveranstaltung)

Dozent: G. Gemmecker      Language: English

Zeit Thursday 12 h - 15 h, starting Thu. Oct. 17, 2019      Ort:   CH 26410

Prüfung: written exam, Wednesday Feb. 26th, 2020, 10.00 - 12.00 h, ATTENTION - ROOM CHANGED: CH 53301

Content:

2D NMR spectroscopy

  • Basic principles of NMR spectroscopy
  • Product operator formalism, principles of 2D NMR
  • 2D pulse sequences for studying structure and conformation of molecules
  • Heteronuclear NMR

Scripts, homework & other material:   (will be added as the lecture progresses)

 Scripts    Tutorials /
 "Homework"
 Solutions NMR spectra

 Advanced_NMR script 2019

 Slides (part 1)

 Slides (part 2)

 Slides (part 1)

                  

 Tutorial 1

 Tutorial 2

 Tutorial 3

 Tutorial 4

 Tutorial 5

 Tutorial 1solutions

 Tutorial 2 solutions

 Tutorial 3 solutions

 Tutorial 4 solutions

 Tutorial 5 solutions

 COSYDF (tar archive)
 COSYDF (PDF file)

 CsA-1H,13C-HSQC (tar file)
 CsA-1H,13C-HSQC (PDF file)

 CsA-1H,13C-HMBC (tar file)
 CsA-1H,13C-HMBC (PDF file)

         

 NEW:   Spindrops

visualization program for NMR
 - try it out!

 

 Workspace files for import into SpinDrops:

 W.1.1_effect_of_rf_field

 W.2.5_chemical_shift

 W.2.6.1_effect_of_pulses_1

 W.2.6.2_effect_of_pulses_2

 W.2.6.3_effect_of_pulses_3

 W.2.7_scalar_coupling

 W.2.8.1_Ialpha

 W.2.8.2_Ibeta

 W.3.0_COSY_transfer

 W.3.1_phase_cycle_COSY

 W.3.2_phase_cycle_DQF-COSY

 (thankfully provided by A. Greiner)

 

 

 

 
 Slides (part 2)    homework 3    
     homework 5  

 1H,13C-HSQC (tar archive, 3 MB) - process yourself!
 1H,13C-HSQC (PDF file)

 1H,13C-HMBC (tar archive, 22 MB)  - process yourself!
 1H,13C-HMBC (PDF file)