Vorlesung "Advanced NMR Spectroscopy"

Lecture Advanced NMR Spectroscopy (Spezielle Aspekte der Organischen Chemie)                           TUMonline

Vorlesung, 2 SWS; Chemie (M.Sc.): HF/NF OC (Wahlpflicht "Spezielle Aspekte der OC"), alle HF/NF (Wahlpflicht)

Dozent: G. Gemmecker

Zeit Monday 10.15 h - ca. 11.50 h, starting Mon Oct. 15, 2018; NO LECTURE on Mon. Nov 5th!

Ort:   CH 27401

Prüfung: written exam on Saturday (!), Feb . 16th 2018, 10:00 h - 11:30 h, room CH 22210

Content:

2D NMR spectroscopy

  • Basic principles of NMR spectroscopy
  • Product operator formalism, principles of 2D NMR
  • 2D pulse sequences for studying structure and conformation of molecules
  • Heteronuclear NMR

Scripts, homework & other material:   (will be added as the lecture progresses)

 Scripts    Tutorials /
 "Homework"
 Solutions NMR spectra

 Advanced_NMR script 2018 (part 1)

 NMR history

 Slides (part 1)

                  

 homework 1

 homework 2

solutions 1

 COSYDF (tar archive)
 COSYDF (PDF file)

         

 NEW:   Spindrops

visualization program for NMR
 - try it out!

 

 Workspace files for import into SpinDrops:

 W.1.1_effect_of_rf_field

 W.2.5_chemical_shift

 W.2.6.1_effect_of_pulses_1

 W.2.6.2_effect_of_pulses_2

 W.2.6.3_effect_of_pulses_3

 W.2.7_scalar_coupling

 W.2.8.1_Ialpha

 W.2.8.2_Ibeta

 W.3.0_COSY_transfer

 W.3.1_phase_cycle_COSY

 W.3.2_phase_cycle_DQF-COSY

 (thankfully provided by A. Greiner)

 

 

 

 
 Slides (part 2)    homework 3    
     homework 5  

 1H,13C-HSQC (tar archive, 3 MB) - process yourself!
 1H,13C-HSQC (PDF file)

 1H,13C-HMBC (tar archive, 22 MB)  - process yourself!
 1H,13C-HMBC (PDF file)