Vorlesung "Advanced NMR Spectroscopy"

Lecture Advanced NMR Spectroscopy                          TUMonline

Vorlesung, 3 SWS / 5 ECTS; Chemie (M.Sc.): Schwerpunkt OC (Wahlpflicht), alle HF/NF (Wahlveranstaltung)

Lecturer: G. Gemmecker      Language: English

Time:   Thursday, 12.15 h, seminar room CH26410; start Oct. 21st, 2021 (no lecture on Dec 23rd, 2021);
            due to construction work, we will be in CH26411 in the first week (Thu. 21st. Oct. 2021)!
            last years lecture will be made available in Moodle for self-learning
            (attention: depending on incidence / Covid rules, the lecture might switch to Zoom mode at any time!)

Examination:    written exam (Feb. 2022)

Content:   2D NMR spectroscopy

  • Basic principles of NMR spectroscopy
  • Product operator formalism, principles of 2D NMR
  • 2D pulse sequences for studying structure and conformation of molecules
  • Heteronuclear NMR

Scripts, homework & other material:   script, exercises etc. are available via Moodle or from below

 

Additional material (will be added during the course):

 Scripts    Tutorials /
 "Homework"
 Solutions NMR spectra to play with

 Advanced_NMR_Script_2020_1-2

 Advanced_NMR_Script_2020_3

 Advanced_NMR_Script_2020_4

 Advanced_NMR_Script_2020_5

 

  Tutorial_1

  Tutorial_2

  Tutorial_3

  Tutorial_4

  Tutorial_5

  Tutorial_6

  Tutorial_1_solutions

  Tutorial_2_solutions

  Tutorial_3_solutions

  Tutorial_4_solutions

  Tutorial_5_solutions

  Tutorial_6_solutions

 COSYDF (tar archive) 
 COSYDF (PDF file)

 CsA-1H,13C-HSQC (tar file) 
 CsA-1H,13C-HSQC (PDF file)

 CsA-1H,13C-HMBC (tar file) 
 CsA-1H,13C-HMBC (PDF file)

 1H,13C-HSQC (tar archive, 3 MB) - process yourself!
 1H,13C-HSQC (PDF file)

 1H,13C-HMBC (tar archive, 22 MB)  - process yourself!
 1H,13C-HMBC (PDF file)

         

 NEW:   Spindrops

visualization program for NMR
 - try it out!

 

 Workspace files for import into SpinDrops:

 W.1.1_effect_of_rf_field

 W.2.5_chemical_shift

 W.2.6.1_effect_of_pulses_1

 W.2.6.2_effect_of_pulses_2

 W.2.6.3_effect_of_pulses_3

 W.2.7_scalar_coupling

 W.2.8.1_Ialpha

 W.2.8.2_Ibeta

 W.3.0_COSY_transfer

 W.3.1_phase_cycle_COSY

 W.3.2_phase_cycle_DQF-COSY

 (thankfully provided by A. Greiner)